3.2 mm HXY low E field H13900
Probe description: PH MASDVT 850W6 BL3.2 X/Y/H LLC
Probe Test Results (Stated 90o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)
Insert 13C/15N:
Nuc | 90o pulse |
Pulse power |
Pulse power (W) |
Configuration 13C/15N |
Sample | Remarks |
79Br | 5.2 | -.9 | 360 | λ/4 | KBr | |
13C | 5.6 | -1.2 | 400 | λ/4 | Adamantane | line width 5.2Hz |
1H | 2.7 | -2.24 | 300 | λ/4 | Adamantane | |
13C | 5.6 | -1.2 | 400 | λ/4 | Glycine (CP) | S/N 36 (ns=4) |
1H | 2.43 | -2 | 283 | λ/4 | Glycine | acq for 50ms decoupling |
15N | 9 | -1.53 | 500 | λ/4 | Glycine |
DR mode
Nuc | 90o pulse |
Pulse power |
Pulse power (W) |
Configuration |
Sample | Remarks |
79Br | 3.5 | -0.9 | 360 | λ/2 | KBr | |
1H | 3.5 | .7 | 152 | λ/2 | Adamantane | |
13C | 3.6 | -1.2 | 402 | λ/2 | Adamantane | |
13C | 3.7 | 0 | 305 | λ/2 | Glycine (CP) | S/N 61 (ns=4) |
1H | 2.42 | -2 | 283 | λ/2 | Glycine (CP) |
Tuning range (measured on the bench, double resonnace mode 1H-X )
λ/2 mode |
151.5→281 MHz |
Includes: 199Hg(152.242), 77Se(162.108), 29Si(168.871), 127I(170.064), 207Pb(177.825), 111Cd( 180.332), 165Ho(181.390), 195Pt(182.723), 113In(185.859), 115In(186.257), 113Cd(188.642), 99Tc(191.321), 185Re(191.459), 187Re(193.389), 59Co(201.680), 121Sb(203.410), 69Ga(204.012), 159Tb(204.340), 45Sc(206.480), 93Nb(208.047), 55Mn(210.708), 151Eu(211.310), 79Br(212.959), 13C(213.733), 27Al(221.483), 123Te(222.443), 51V(223.575), 23Na(224.841), 63Cu(225.382), 81Br(229.555), 129Xe(236.387), 65Cu(241.431), 71Ga(259.222), 141Pr(260.270), 125Te(268.173), 11B(272.714), 115Sn(278.109), 87Rb(278.124) |
λ/4 mode |
55→217 MHz |
Includes: 95Mo(55.394), 201Hg(56.198), 97Mo(56.556), 43Ca(57.205), 14N(61.424), 33S(65.246), 189Os(66.006), 21Ne(67.102), 176Lu(69.114), 37Cl (69.324), 131Xe(70.073), 169Tm(70.465), 61Ni (75.956), 91Zr(79.019), 85Rb( 82.067), 35Cl (83.282), 135Ba( 84.443), 50V( 84.748), 15N( 86.163), 10B(91.321), 153Eu( 93.330), 137Ba( 94.460), 175Lu(96.934), 181Ta( 101.912), 123Sb( 110.153), 133Cs(111.487), 138La(112.152), 17O(115.230), 9Be( 119.440), 139La(120.068), 6 Li(125.087), 2H(130.480), 209Bi(136.589), 75As(145.542), 171Yb(148.744), 199Hg(152.242), 77Se(162.108), 29Si(168.871), 127I(170.064), 207Pb( 177.825), 111Cd( 180.332), 165Ho(181.390), 195Pt(182.723), 113In(185.859), 115In(186.257), 113Cd(188.642), 99Tc(191.321), 185Re(191.459), 187Re(193.389), 59Co(201.680), 121Sb(203.410), 69Ga(204.012), 159Tb(204.340), 45Sc(206.480), 93Nb(208.047), 55Mn(210.708), 151Eu(211.310), 79Br(212.959), 13C(213.733), |